Solid-state NMR (Record no. 49896)

000 -LEADER
fixed length control field 05610nam a2200649 4500
001 - CONTROL NUMBER
control field 9781606503522
003 - CONTROL NUMBER IDENTIFIER
control field NYMP
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20190704130046.0
006 - FIXED-LENGTH DATA ELEMENTS--ADDITIONAL MATERIAL CHARACTERISTICS
fixed length control field m eo d
007 - PHYSICAL DESCRIPTION FIXED FIELD--GENERAL INFORMATION
fixed length control field cr cn |||m|||a
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 120913s2012 nyua foab 001 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number 9781606503522 (electronic bk.)
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number 1606503529 (electronic bk.)
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
Canceled/invalid ISBN 9781606503508 (print)
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
Canceled/invalid ISBN 1606503502 (print)
024 7# - OTHER STANDARD IDENTIFIER
Standard number or code 10.5643/9781606503522
Source of number or code doi
035 ## - SYSTEM CONTROL NUMBER
System control number (OCoLC)809804677
035 ## - SYSTEM CONTROL NUMBER
System control number (CaPaEBR)10588196
035 ## - SYSTEM CONTROL NUMBER
System control number (CaBNvSL)swl00401257
040 ## - CATALOGING SOURCE
Original cataloging agency CaBNVSL
Transcribing agency CaBNVSL
Modifying agency CaBNVSL
050 #4 - LIBRARY OF CONGRESS CALL NUMBER
Classification number QD96.N8
Item number A668 2012
082 04 - DEWEY DECIMAL CLASSIFICATION NUMBER
Classification number 543.0877
Edition number 23
100 1# - MAIN ENTRY--PERSONAL NAME
Personal name Apperley, David C.
9 (RLIN) 121311
245 10 - TITLE STATEMENT
Title Solid-state NMR
Medium [electronic resource] :
Remainder of title basic principles & practice /
Statement of responsibility, etc. David C. Apperley, Robin K. Harris & Paul Hodgkinson.
260 ## - PUBLICATION, DISTRIBUTION, ETC.
Place of publication, distribution, etc. [New York, N.Y.] (222 East 46th Street, New York, NY 10017) :
Name of publisher, distributor, etc. Momentum Press,
Date of publication, distribution, etc. 2012.
300 ## - PHYSICAL DESCRIPTION
Extent 1 electronic text (xiv, 276 p.) :
Other physical details ill., digital file.
500 ## - GENERAL NOTE
General note English ebook
500 ## - GENERAL NOTE
General note ebook
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Includes bibliographical references and index.
505 0# - FORMATTED CONTENTS NOTE
Formatted contents note Preface -- About the authors --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 1. Introduction -- 1.1 The utility of NMR -- 1.2 A preview of solid-state NMR spectra -- 1.3 The solid state -- 1.4 Polymorphism, solvates, co-crystals & host:guest systems -- 1.5 NMR of solids & the periodic table --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 2. Basic NMR concepts for solids -- 2.1 Nuclear spin magnetization -- 2.2 Tensors -- 2.3 Shielding -- 2.4 Indirect coupling -- 2.5 Dipolar coupling -- 2.6 Quadrupolar coupling -- 2.7 Magic-angle spinning -- 2.8 Relaxation --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 3. Spin-1/2 nuclei: a practical guide -- 3.1 Introduction -- 3.2 The vector model & the rotating frame of reference -- 3.3 The components of an NMR experiment -- 3.4 Cross polarization -- 3.5 High-resolution spectra from 1H (& 19F) --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 4. Quantum mechanics of solid-state NMR -- 4.1 Introduction -- 4.2 The Hamiltonians of NMR -- 4.3 The density matrix -- 4.4 Density operator treatments of simple NMR experiments -- 4.5 The density matrix for coupled spins -- 4.6 Euler angles & spherical tensors -- 4.7 Additional analytical tools --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 5. Going further with spin-1/2 solid-state NMR -- 5.1 Introduction -- 5.2 Linewidths in solid-state NMR -- 5.3 Exploiting indirect (J) couplings in solids -- 5.4 Spectral correlation experiments -- 5.5 Homonuclear decoupling -- 5.6 Using correlation experiments for spectral assignment -- 5.7 Further applications --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 6. Quadrupolar nuclei -- 6.1 Introduction -- 6.2 Characteristics of first-order quadrupolar spectra -- 6.3 First-order energy levels & spectra -- 6.4 Second-order zero-asymmetry cases -- 6.5 Spectra for cases with non-zero asymmetry: central transition -- 6.6 Recording one-dimensional spectra of quadrupolar nuclei -- 6.7 Manipulating the quadrupolar effect -- 6.8 Spectra for integral spins --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 7. Relaxation, exchange & quantitation -- 7.1 Introduction -- 7.2 Relaxation -- 7.3 Exchange -- 7.4 Quantitative NMR -- 7.5 Paramagnetic systems --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note 8. Analysis & interpretation -- 8.1 Introduction -- 8.2 Quantitative measurement of anisotropies -- 8.3 Measurement of dipolar couplings -- 8.4 Quantifying indirect (J) couplings -- 8.5 Tensor interplay -- 8.6 Effects of quadrupolar nuclei on spin-1/2 spectra -- 8.7 Quantifying relationships between tensors -- 8.8 NMR crystallography --
505 8# - FORMATTED CONTENTS NOTE
Formatted contents note Appendices -- A. The spin properties of spin-1/2 nuclides -- B. The spin properties of quadrupolar nuclides -- C. Liouville space, relaxation & exchange -- C.1 Introduction to Liouville space -- C.2 Application to relaxation -- C.3 Application to chemical exchange -- D. Introduction to solid-state NMR simulation -- D.1 Specifying the spin system -- D.2 Specifying the powder sampling -- D.3 Specifying the pulse sequence -- D.4 Efficiency of calculation -- Index.
506 ## - RESTRICTIONS ON ACCESS NOTE
Terms governing access Restricted to libraries which purchase an unrestricted PDF download via an IP.
520 3# - SUMMARY, ETC.
Summary, etc. Nuclear magnetic resonance (NMR) has proved to be a uniquely powerful and versatile spectroscopy, and no modern university chemistry department or industrial chemistry laboratory is complete without a suite of NMR spectrometers. The phenomenon of nuclear spin may seem an odd basis for an analytical tool, but it is the relative isolation of the nuclear spin from its surroundings that makes it an ideal noninterfering probe of the electronic environment. Different sites are clearly identified by their chemical shifts, while J couplings in 1H spectra provide connectivity information. The combination of these two complementary interactions, plus the formidable array of different NMR experiments developed since the arrival of Fourier transform NMR in 1966, has revolutionized the practice of chemistry.
530 ## - ADDITIONAL PHYSICAL FORM AVAILABLE NOTE
Additional physical form available note Also available in print.
538 ## - SYSTEM DETAILS NOTE
System details note Mode of access: World Wide Web.
538 ## - SYSTEM DETAILS NOTE
System details note System requirements: Adobe Acrobat reader.
588 ## - SOURCE OF DESCRIPTION NOTE
Source of description note Title from PDF t.p. (viewed on September 13, 2012).
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Nuclear magnetic resonance spectroscopy.
9 (RLIN) 215
653 ## - INDEX TERM--UNCONTROLLED
Uncontrolled term Solid-state NMR
653 ## - INDEX TERM--UNCONTROLLED
Uncontrolled term Magic-angle spinning
653 ## - INDEX TERM--UNCONTROLLED
Uncontrolled term Solid-state structure
653 ## - INDEX TERM--UNCONTROLLED
Uncontrolled term NMR crystallography
653 ## - INDEX TERM--UNCONTROLLED
Uncontrolled term Cross polarization
653 ## - INDEX TERM--UNCONTROLLED
Uncontrolled term Quadrupolar nuclei
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Harris, Robin K.
Fuller form of name (Robin Kingsley)
9 (RLIN) 121312
700 1# - ADDED ENTRY--PERSONAL NAME
Personal name Hodgkinson, Paul.
9 (RLIN) 121313
776 08 - ADDITIONAL PHYSICAL FORM ENTRY
Relationship information Print version:
International Standard Book Number 1606503502
-- 9781606503508
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier http://portal.igpublish.com/iglibrary/search/MPB0000073.html

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